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Chemistrystudents.leeds.ac.uk

Year: 2013-14
Name:
1. AMANTADINE (MChem only
)

(i) N-(1-Adamantyl)acetamide
Phys App
(5) NMR(spec)
(15) NMR(assign)
Mechanism

(ii) Amantadine
Phys App
(10) NMR(spec)
(5) NMR(assign)
Mechanism
(10) Questions (3)

2. CHIRAL EPOXIDATION
(i) (3S,4R)-2,2-Dimethyl-3,4-epoxy-6-pentafluoroethyl-2H-1-benzopyran
Phys App.
(20) NMR(spec)
(10) NMR(assign)
(10) [α]D
Mechanism
Year: 2013-14
Name:

(ii) (3S,4R)-2,2-Dimethyl-4-(2-oxopiperidin-1-yl)-6-pentafluoroethyl-2H-1-benzopyran-3-ol
Phys App.
(15) NMR(spec)
(15) NMR(assign)
(5) [α]D
(10) Questions (4)
Mechanism

3. IBUPROFEN
(i) 4-Isobutylisopropenylbenzene
Phys App
(15) NMR(spec)
(15) NMR(assign)
Mechanism

(ii)(S)-2-(4-Isobutylphenyl)-1,2-diol
Phys App
(15) NMR(spec)
(5) NMR(assign)
Mechanism
Year: 2013-14
Name:

(iii)(S)-2-(4-Isobutylphenyl)-propanol
Phys App
(15) NMR(spec)
(10) NMR(assign)
Mechanism

(iv) (S)-Ibuprofen
Phys App
(15) NMR(spec)
(5) NMR(assign)
(10) [α]D
Mechanism
(10) Questions (3)

4. NITRAZEPAM
(i) 1-Bromoacetamido-5-nitrobenzophenone
Phys App
(5) NMR(spec)
(10) NMR(assign)
Mechanism
Year: 2013-14
Name:

(ii) 2-Azidoacetamido-5-nitrobenzophenone
Phys App
(15) NMR(spec)
(5) NMR(assign)
Mechanism

(iii) Nitrazepam
Phys App
(10) NMR(spec)
(5) NMR(assign)
Mechanism
(10) Questions

(iv) Rationalisation of the NMR using molecular modelling
Modelling exercise
Year: 2013-14
Name:

5. FLUOXETINE
(i)R-(+)-3-Chloro-1-phenylpropan-1-ol
Phys App
(15) NMR(spec)
(5) NMR(assign)
(10) [α]D
Mechanism

(ii) R-(-)-3-Iodo-1-phenylpropan-1-ol
Phys App
(15) NMR(spec)
(15) NMR(assign)
(15) [α]D
Mechanism

(iii) R-(-)-3-N-Methylamino-1-phenylpropan-1-ol
Phys App
(15) NMR(spec)
(15) NMR(assign)
Mechanism
Year: 2013-14
Name:

(iv) a. R-(+)-Fluoxetine, (v) b. R-(+)-Fluoxetine hydrochloride
Phys App
(10+10) IR (b)
(10+10) NMR(spec)
(5) NMR(assign)
(10) Questions (2)
Mechanism
(5) [α]D

6. PROPRANOLOL (MChem only
)
(i) (2R)-Glycidyl tosylate
Phys App
(15) NMR(spec)
(5) NMR(assign)
Mechanism

(ii) (2R)-Glycidyl naphthyl ether
Phys App
(15) NMR(spec)
(15) NMR(assign)
Mechanism
Year: 2013-14
Name:

(iii) (2S)-Propranolol
Phys App
(15) NMR(spec)
(15) NMR(assign)
Mechanism

(iv) (2S)-Propranolol hydrochloride
Phys App
(15) NMR(spec)
(5) NMR(assign)
(10) [α]D
Mechanism
(10) Questions (2)

ANALYTICAL EXERCISES


COMMENTS (Illness, absences, etc.)

Source: http://www.chemistrystudents.leeds.ac.uk/fileadmin/user_upload/Current__Students/MEDICINAL_CHEMISTRY_level_3_mark_sheet_blank.pdf

Translation_sidorin-

/Translated from Russian to English/ /Stamp: DEPARTMENT OF HEALTH OF MOSCOW CITYSCIENTIFIC & PRACTICAL CENTER OF MEDICAL CARE FOR CHILDREN WITH CONGENITAL ABNORMALITY OF CRANIOFACIAL AREA AND INHERENT DISEASES CASE RECORD Nr. 622/10 Full name : Sidorin Georgy Vasilievich Age : 2 years old 7 month Date of birth : 09.07.2007 Settlement : Moscow city He stayed at Psychoneurolog

The study of cardiac function during anesthesia by phonocardiogram

JOURNAL OF ELECTRONIC SCIENCE AND TECHNOLOGY OF CHINA, VOL. 6, NO. 1, MARCH 2008 Effect of Mixed Anesthesia on Cardiac Function by Phonocardiogram Fei Han, Hong-Mei Yan, Xin-Chuan Wei, and Qing Yan Abstract ⎯ Objective of this investigation is to further testing are highly consistent and strongly suggestive of analyze the cardiac function status change by phonocar- changes i

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